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Synthesis, crystal structure and characterisation of two crystals of 5-[4 ''-(bromomethyl)biphenyl-2-yl]-2-trityl-2H-tetrazole
作者:Jing Zhao, Yang-hui Wang, Ming Lou and Bai-wang Sun*
關鍵字:synthesis, polymorph, different solvent, crystal structure
論文來源:期刊
發表時間:2013年
Two polymorphs of 5-[4’-(bromomethyl)biphenyl-2-yl]-2-trityl-2H-tetrazole can be characterised by single-crystal X-ray diffraction and Hirschfeld surface analysis. Both polymorphs crystallise in the monoclinic space group P21/c, but their cell parameters are different. The interatomic distances of phase A and B are different, and the arrangements of the dipolymers in phase A and B are remarkably different for the molecular orientation and interatomic distances according to their different  π…π  stacking interactions. Additionally, the size and shape of a Hirschfeld surface also reflects the interplay between different atoms and intermolecular contacts in a crystal. From the Hirschfeld surfaces of phase A and B, we can interpret the different proportions of interaction.
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