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VARTM Process for Ramie Fiber Fabric Reinforced Anionic Polyamide-6 Composites

資料類型：

PDF文件

關鍵詞：

vartm anionic polyae-6 ramie fiber fabric thermoplastic
composites

資料大小：

109K

所屬學科：

分子表征

來源：

第六屆亞歐研討會上處理和性能增強聚合物會議文集（2013.6.2-6 武漢）

簡介：

Textilefiberreinforcedthermoplasticcompositesareincreasinglyusedformanufacturinghigh-performancelight-weightstructuresin,forinstance,theaerospaceandautomotiveindustry.Sincetheviscosityofthermoplasticpolymermeltsistoohigh,apoorimpregnationormoldfillwouldbehappened.Inordertomanufacturelarger,thickerandmoreintegratedthermoplasticcompositesthancurrentlycanbeachievedbymeltprocessing,avacuumassistedresintransfermolding(VARTM)iscurrentlybeingdevelopedusingareactivethermoplasticpolymercalledanionicpolyamide-6(APA-6).Naturalfiber,asakindoflowcost,lightweight,highspecificstrengthandstiffness,andnaturaldegradationofenvironment-friendlymaterial,usedinreinforcedcompositesiswidelyconcerned.However,nonaturalfiberreinforcedreactivethermoplasticpolymergradeshavebeenpreparedsofar.Throughourpreviousstudies,itwasdemonstratedthattherewasastronginteractionbetweenthelargenumberofhighlyreactivehydroxylonthesurfaceofcelluloseandtheinitiatorofAPA-6,whichresultinincompletepolymerizationwhenputtogether.Inordertosolvetheproblem,amethodwasadoptedbyusinganew-styleinitiatorcalledcaprolactammagnesiumbromide,whichhaslowerreactivityandweakeralkalineduetothefactthatitscationislargerandlessacidic,thuslimitedthereactionwiththehydroxylgroupsonthecellulose.itwouldmarkedlyreducetheconsumptionoftheinitiator.Asaresult,theroleofinhibitorhasbeensignificantlyimproved.FollowingramiefiberfabricreinforcedAPA-6compositeswithanaveragethicknessof2.5mmwaspreparedbyVARTM.Thesoxhletextractionanddifferentialscanningcalorimeter(DSC)measurementsrespectivelysuggestedthedegreeofconversionandcrystallizationofcompositeswas94%and50%.Remarkableimprovementofmechanicalpropertieswasachievedthroughdynamicmechanicalanalysis(DMA)andthree-pointbendingtest.Favorableinterfacialadhesionandwettabilitywererevealedbyscanningelectronmicroscopy(SEM)observation.Thevoidcontentandfiberfractionofcompositesweremeasuredbydensimeter.

作者：

M. B. Yang, Z. Kan

上傳時間：

2013-06-26 15:37:56

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